manuais Axis BTA 2100D

Axis BTA 2100D Manual do Operador (597 páginas)

Marca: Axis | Categoria: Software | Tamanho: 4.63 MB |

Índice

Operation Manual

Contents

Getting Started

MS Workstation Toolbar

Button

Application Buttons

Quick Link Buttons

Move to Windows Taskbar

Application Descriptions

Small Buttons on Toolbar

2000 MS Module Control

Network

Company Network)

Server]

Click Setup

2000 MS Instrument Control

2000 Module Window

Manual Control

Instrument Settings

Setpoints tab

Adjustments tab

Auto Tune

Set Points

Temperatures

Diagnostics Mode

System Test

Monitor Window

Shutdown Mode

Acquisition Mode

2000 MS Instrument Window

Inject Single Sample Menu

Saturn Module Keypad Dialog

Spectrum Toolbar

Status and Control Window

Operating Conditions

SetPoints

Adjustments

See the Chemical Ionization

Autotune Mode

Control and Status

Method and Set Points

Auto Tune Checks

Air/Water Check

Electron Multiplier Tune

Mass Calibration

Trap Function Calibration

Temperatures Mode

Diffusion Pump Shutdown

Diffusion Pump Startup

Acquisition

Electron Multiplier Gain

Axial Modulation

Emission Current

Ion Trap Temperature

AGC Target TIC Value

100

The Instrument Window

101

Overview

109

Specifying a RecalcList

112

Using QuickStart

113

3800 GC Injecting Multiple

115

Samples

115

Using the Sequence Window

122

Adjust time scale

130

Select Edit Module Info

131

3900 GC Injecting Multiple

139

System Control Menus

147

Edit Menu

148

Inject Menu

149

Automation Menu

149

Recalculate Menu

150

Instrument Menu

150

Windows Menu

151

Help Menu

152

System Control Toolbar

153

2000 MS Method Basic Scan

155

Functions

155

2000 MS Method Chemical

157

Ionization

157

The CI Parameters

160

Ejection Amplitude (v)

161

Background mass

161

Target TIC Value

161

Maximum ionization time

161

Maximum reaction time

161

Prescan Ionization Time

162

Using Liquid CI Reagents

164

Choice of Liquid CI Reagents

165

Than Methane

167

Tuning for CI Operation

168

Recommended Reading

169

2000 MS Method Command

171

Reference

171

The flow sampling segment

172

Ionization Mode

173

Ion Preparation

173

Segment Setpoints

174

Ionization Mode - EI Auto

175

Ionization Mode - EI Fixed

176

CI Fixed Parameters

178

Ion Storage (SIS) Parameters

179

Customize SIS

179

The MS/MS Ion Prep Method

180

Item Description

181

Customize Resonant Method

182

Ion Preparation MS/MS

185

2000 MS Method Electron

191

Ion Formation

192

AGC Prescan

192

Mass Scanning

193

Software Parameters

195

Mass Range Segment Breaks

197

Ionization Storage Level

197

Ionization Time Factor

197

Maximum Ionization Time

198

Background Mass

198

The Ion Preparation Method

201

Autoscale Waveform

206

Tips for Using SIS

207

Theory of Operation

209

Parent Ion Isolation

210

Product Ion Formation

210

Product Ion Mass Scanning

213

Chemical Ionization

213

Control

213

Summary

213

The MS “q” Calculator

216

Isolation

217

Dissociation

220

Excitation amplitude (volts)

224

Parent ion

224

Product ion 1

224

Product ion 2

224

Using Nonresonant Excitation

225

MS/MS/MS

226

2000 MS Method Section

229

The Method Builder Window

232

The 2000 MS Method Windows

233

The Flow Sampling Segment

235

The Startup Method

237

Status Window

238

Importing Method Sections

239

Deleting Method Sections

240

Printing the Method

241

Password Protecting a Method

241

3800 GC Method Command

243

Default Clean Section

244

Clean Mode Section

245

Internal Standard Section

246

Solvent Plug Settings

247

User Defined Settings

248

Viscosity Settings

248

3800 GC Sample Delivery

250

3800 GC Injector

251

1061 Injector

252

1079 Injector

252

Spilt Ratio Dialog Box

253

3800 GC Flow/Pressure

255

Type 4 (for valved systems)

257

3800 GC Column Oven

258

3800 GC Detector

259

FID Detector

260

TCD Detector

261

TSD Detector

262

ECD Detector

264

PFPD Detector

265

Methanizer Dialog Box

266

3800 GC Output

267

3800 GC Data Acquisition

268

3800 GC Method Section

269

MS Workstation

270

The 3800 GC Method Windows

273

Spreadsheet editing

274

Checking Method End times

275

Sample Delivery Window

276

Injector Window

278

1177 Injector

280

1041 Injector

281

SPT Injection Device

282

Flow/Pressure Window

283

Pressure spreadsheet

286

Flow spreadsheet

286

Column Oven Window

287

Detector Window

288

Micro-TCD Detector

292

Output Window

296

Data Acquisition Window

297

Autosampler Window

298

Hardware

299

3800 GC System Control

305

Command Reference

305

3800 Operation Display

306

Temp Zones Status Display

307

Component Status Display

307

Column Oven Status:

308

AutoSampler Status:

309

Sample Delivery Status:

310

Name Default State Energized

310

1041/1061 Injector Status:

312

SPT Injector Status:

313

FID Status:

317

ECD Status:

319

TSD Status:

319

PFPD Status:

320

8400/8410 Carrousel Display

324

Chromatogram Display Toolbar

325

3800 Setup Dialog Box

326

Field Description

328

3900 GC Method Command

335

3900 GC Injector Section

343

Type 1 (for 1177 injector)

345

3900 GC Column Oven Section

346

3900 GC Method Section

347

The 3900 GC Method Windows

351

GC Control Window

354

Injector Section

355

Column Oven Section

357

3900 GC System Control

365

Oven Status Display

367

Injector EFC Status Display

368

3900 Setup Dialog Box

369

8200 AutoSampler Instrument

383

Control Command Reference

383

Hardware Dialog Box

386

Automix Routines Dialog Box

387

Carrousel Dialog Box

389

8200 Configuration Window

391

Liquid Sampling Options

392

User Defined Parameters

393

SPME Options

394

Main Toolbar

399

Print Setup Dialog Box

402

Edit Notes Dialog Box

403

RecalcList Window

404

Open Data File Dialog Box

409

SampleList Window

410

Sequence Window

416

Automation File Editor

417

GC Batch Report

427

Method Selection

428

Generating Reports

429

Changing Report Commands

429

GC Data Handling Calibration

431

Automated Calibration

432

Select View Curves

435

Calibration Verification

436

Introduction

437

Performing a Pilot Run

437

Peak Detection

438

Rejecting Solvent Peaks

439

Skimming Fused Peaks

439

Splitting Fused Peaks

440

Forcing Peaks

440

Identifying Peaks

441

Building a Calibration Curve

441

Choosing a Calibration Type

443

GC Data Handling Method

445

Peak Table

447

Calibration Setup

449

Coefficients Table

451

Calibration Curve Window

452

This Report Only Dialog Box

453

Print All Dialog Box

454

Overlay Window

454

Point Info Dialog Box

455

Coefficients Dialog Box

455

Verification Setup

456

Time Events Table

457

Time Events

458

Event Description

459

Run Information

463

Open Method File Dialog Box

464

Save Method As Dialog Box

466

Preferences Dialog Box

467

Layout Tab

468

Trace Settings Tab

469

Offsets Tab

471

Colors Tab

472

Fill Peak Table Window

475

Exact View Dialog Box

476

File Menu

477

View Menu

478

Results Menu

479

Edit Method Menu

480

Toolbar Overview

483

Method Quick Link Toolbar

484

Chromatogram Toolbar

484

Locator Window

487

Main Window

488

Opening Data Files

489

Zooming and Scrolling

489

Autoscaling

490

Moving Baselines

490

Info-Panels

491

Cursor Info-Panel

492

Run File Info-Panel

492

Visual Method Edit Window

493

Types of Time Events

494

Right Mouse Menus

496

Action Effect of Action

497

GC Interactive Graphics

499

The Locator Window

500

Changing Viewing Options

503

The Preferences Dialog Box

504

Offsets

505

Selecting a Method

506

Integration Parameters

509

Filling the Peak Table

512

These events are selected

514

Calculating Results

515

Viewing Results

517

Viewing Calibration Curves

518

GC Standard Report Method

521

Results Format

523

Chromatogram Format

524

Print Options

527

Automated Report Generation

530

Select Printer Setup

531

Specify a Print action

532

Select the Data File

534

Method Builder Dialog Boxes

537

Add Password Dialog Box

540

Change Password Dialog Box

541

Star Assistant Wizard

545

Select Configuration

546

Configure Modules

547

Confirm Configuration

550

Method Builder Menus

551

Window Menu

552

Method Builder Toolbars

555

Directory Toolbar

556

Window Toolbar

557

Method Builder Window

559

Method Directory

560

Method Parameters

561

Module Information Editor

563

Creating a Section

564

Deleting a Section

564

Renaming a Section

564

Adding an Entry to a Section

565

Commands

567

Dialog Boxes

568

Security Administration

571

Application Locking

573

File Revision Settings

574

Standard GC Reports Command

577

Options Menu

578

Print Dialog Box

582

Printer Setup Dialog Box

583

Title Dialog Box

583

Results Options Dialog Box

586

Find Dialog Box

587

Standard GC Reports Format

589

Descriptions

589

Verification Report

595

Standard GC Reports Toolbar

597

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Axis BTA 2100D Manual do Operador (597 páginas)

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